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Reagent for CALDUR® Manganese – Colorimetric:
See also:
CALDUR® Manganese Test Set – Colorimetric
What is manganese measured for?
Manganese (Mn) is a naturally occurring heavy metal that is frequently found in groundwater and surface waters. The limit value for drinking water is 0.05 mg/l Mn (Drinking Water Ordinance).
Elevated manganese concentrations lead to black-brown deposits in pipes, discoloration of the water and a metallic taste. In waterworks, manganese must be reliably removed, as even low concentrations can lead to operational disruptions.
Manganese can cause deposits and corrosion in cooling water systems and industrial treatment. Regular monitoring is therefore essential.
How does the test set work?
The CALDUR® Manganese Test Set – Colorimetric is based on the formaldoxime method. After adding three reagents to the water sample, a colored complex is formed within 10 minutes, the intensity of which is proportional to the manganese concentration.
The measured value is determined by direct color comparison with a supplied color chart.
Advantages of the CALDUR® test set
Sensitive measuring range 0.03 – 1.0 mg/l Mn
Already detects concentrations below the drinking water limit value
100 provisions per set
Economical for regular checks
Proven formaldoxime method
Selective for manganese, low interference
Easy handling with color card
Fast on-site determination without measuring devices
Robust plastic housing with hinged lid
Safe transportation and protection of reagents
Areas of application
Pond / lake
Groundwater / well water
Drinking / tap water
Aquaristics
Pool / Swimming pool
Industrial processing
Boiler water
Food preparation
Waste water treatment
Carrying out the measurement:
Fill water sample into test tubes up to the 10 ml mark
Add 5 drops of reagent A and mix
Add 5 drops of reagent B and mix
Add 3 drops of reagent C and mix
Wait for 10 minutes reaction time
Perform color comparison with color chart
Tip for best results
The sample should be measured immediately after collection, as dissolved manganese(II) can be oxidized to manganese(IV) on contact with atmospheric oxygen and then precipitates as brown manganese oxide. Do not filter Truebe samples before measurement if the total manganese content is to be determined.
Important notes
Measure the sample immediately after taking it – manganese oxidizes in the air
Adhere exactly to the reaction time of 10 minutes
Avoid direct sunlight during the measurement
Iron >5 mg/l can interfere with the measurement
Thoroughly rinse the test tube with the sample before each measurement
Read intermediate values:
If the color lies between two fields, you can form the mean value
(e.g. between 0.1 and 0.2 mg/l = approx. 0.15 mg/l).
Number of possible destinations
You can carry out 100 measurements with one CALDUR® Manganese Test Set.
This refers to the quantity of reagents contained.
Measuring accuracy and reproducibility
Readability: ± 1 color level Reproducibility: Very good if the application instructions are followed Interference: Iron in high concentrations (>5 mg/l) can influence the result. If samples are heavily colored (e.g. by humic substances), the color reading may be more difficult. In these cases, a photometric determination is recommended.
What to do if measured values are out of range?
Measured value > 1.0 mg/l
Verduction
Execution
Calculation of the measured value
1:1
5 ml sample + 5 ml manganese-free water
Measured value × 2
1:4
2 ml sample + 8 ml manganese-free water
Measured value × 5
Measured value < 0.03 mg/l
The measured value is below the detection limit. This is a good result for drinking water, as the limit value of 0.05 mg/l is safely adhered to.
3 reagent bottles (reagent A, reagent B, reagent C) with detailed labeling
1 test tube with 10 ml scale
1 color card with 6 measuring levels
Detailed operating instructions (DE/EN)
Safety data sheets for all reagents
Robust hinged lid box (103 x 91 x 36 mm)
Reagent details
Reagent
Volume
Shelf life
Notes
Reagent A (Formaldoxime)
30 ml
24 months (24M)
Formaldoxime reagent, shake before use
Reagent B (buffer)
15 ml
24 months (24M)
Alkaline buffer solution
Reagent C (oxidizing agent)
10 ml
24 months (24M)
Oxidizing reagent, shake before use
Shelf life: The shelf life starts from the date of manufacture (printed on the bottle).
After opening, the reagents should be used within 12 months.
Store the test kit in a dry, cool place (10-25°C) and protected from direct sunlight.
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